Multi Mycotoxin Sample Preparation

QuEChERS Method for Mycotoxins: CrossTOX®

SMART columns with only 3 cm size for fast sample preparation for multi-mycotoxin analysis by LC-MS/MS - suitable for 18 toxins such as aflatoxins B/G OTA, DON, NIV, ZEA, FB1/FB2 and others.

Josef Hauptmann - HiPP GmbH & Co. Vertrieb KG

"Using the new CrossTOX® columns has made our mycotoxin multi-method much more effective, especially in terms of time and the use of consumables."

ANALYSIS RESULTS

Toxins Analysed So Far:

aflatoxine B1, B2, G1, G2, sterigmatocystin, ochratoxin A, fumonisine B1 and B2, deoxynivalenol, nivalenol, 15-acetyl DON, 3-acetyl DON, DON-3-GLC, zearalenon, T-2 and HT-2, citrinin, diacetoxyscirpenol

WRITTEN IN THE CAPINOV LANDERNEAU LABORATORY

"The CrossTOX® SPE column enables us to maintain the trust in our analyses."

Application

The column can be used in manual sample processing (e.g. with a syringe).

Automated with the robotic system FREESTYLE (filling in a vial).

Or fully automated with direct injection in LC-MS/MS. The column is thus ideal for high-throughput laboratories.

Specifications

Format: SMART (length = 3 cm)
LOD (detection limit): B1 0,04 ng/mL, B2 0,04 ng/mL, G1 0,04 ng/mL, G2 0,04 ng/mL, OTA 0,04 ng/mL,
FB1 0,75 ng/mL, FB2 0,75 ng/mL, DON 0,1 ng/mL, ZEA 0,04 ng/mL, T-2 0,05 ng/mL,
HT-2 0,05 ng/mL, Citrinin 0,1 ng/ mL, NIV 0,1 ng/mL, STC 0,1 ng/mL, DAS 1 ng/ mL
Validated matrices: Food (cereals, nuts, dried fruit), feed
Analyte: Aflatoxins B1, B2, G1, G2, sterigmatocystin, ochratoxin A, fumonisine B1 and B2, deoxynivalenol, nivalenol, 15-acetyl DON, 3-acetyl DON, DON-3-GLC, zearalenon, T-2 and HT-2, citrinin, diacetoxyscirpenol
Storage: Room temperature
Shelf life: 24 months from production date
Loading: 0.5 - 3 mL (analog to 0.6 g matrix)
Recovery: ≥ 85%
Packaging: 100 columns / pack, for manual use, order no. 17900
100 columns / pack, for automated use, order no. 17901
Automation: FREESTYLE CrossTOX®